2、2′-亚​甲基-双[4-特​辛​基-6-(2H‑苯​并​三​唑​基-2)]苯酚​的​无​溶剂​合成

源语言标题
(CN106632111) 2、2′-亚​甲基-双[4-特​辛​基-6-(2H‑苯​并​三​唑​基-2)]苯酚​的​无​溶剂​合成
公开号/公开日
CN106632111 A 2017-05-10 [CN106632111] / 2017-05-10
申请号/申请日
2016CN-0856399 / 2016-09-27
发明人
CHENG GUOLIANG;
申请人
WEIHAI JIN WEI CHEMICAL INDUSTRY LIABILITY;
主分类号
IPC分类号
C07D-249/20
摘要
(CN106632111) 本​发明​公开​了​种​通过​无​溶剂​缩合​合成​2、2′-亚​甲基-双[4-特​辛​基-6-(2H‑苯​并​三​唑​基-2)]苯酚(UV‑360)的​方法。其​过程​是:先以​二​正​丙基​胺​和​甲醛​或​多​聚​甲醛​为​原料,在​温度​约​120℃的​条件下​缩合​脱水​合成​二(正​丙基​氨基)甲烷,再​和​2‑(2′‑羟基‑5′‑特​辛​基​苯基)苯​并​三​唑​在​无​溶剂​和​氢氧化钠​的​催化作用​下于​约​160℃缩合​合成​UV‑360。由于​该​方法​不使​用​高沸点​溶剂,克服​了​现有​方法​存在​的​问题,即​二​正​丙基​氨​容易​回收​及​循环使用,且​产品​质量​高。
地址
代理人
代理机构
;
优先权号
2016CN-0856399 2016-09-27
主权利要求
(CN106632111) 1. One 2, 2 '-methylene-bis [4-te xinji-6-(2H-benzotriazole based-2) ] phenol solvent-free synthesis method, in particular di-n-propyl amine and formaldehyde or paraformaldehyde prior to synthesis as a raw material di (n-propyl amino) methane, is reacted with 2-(2'-hydroxy-5 '-te xinji phenyl) benzotriazole in the absence of a solvent through condensation synthesis 2, 2'-methylene-bis [4-te xinji-6-(2H-benzotriazole based-2) ] phenol.
法律状态
(CN106632111) LEGAL DETAILS FOR CN106632111  Actual or expected expiration date=2036-09-27    Legal state=ALIVE    Status=PENDING     Event publication date=2016-09-27  Event code=CN/APP  Event indicator=Pos  Event type=Examination events  Application details  Application country=CN CN201610856399  Application date=2016-09-27  Standardized application number=2016CN-0856399     Event publication date=2017-05-10  Event code=CN/A  Event type=Examination events  Published application  Publication country=CN  Publication number=CN106632111  Publication stage Code=A  Publication date=2017-05-10  Standardized publication number=CN106632111     Event publication date=2017-05-10  Event code=CN/PB01  Event type=Examination events  Publication    Event publication date=2017-06-06  Event code=CN/SE01  Event type=Examination events  ENTRY INTO FORCE OF REQUEST FOR SUBSTANTIVE EXAMINATION
专利类型码
A
国别省市代码
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