(WO2019121394) Polymorphs 机翻标题: 暂无翻译,请尝试点击翻译按钮。

源语言标题
(WO2019121394) Polymorphs
公开号/公开日
WO2019/121394 / 2019-06-27
申请号/申请日
WOEP2018/084957 / 2018-12-14
发明人
GEORGE NEILJONES IANHONE JOHN;
申请人
SYNGENTA PARTICIPATIONS;
主分类号
IPC分类号
A01N-043/80 C07D-261/04
摘要
(WO2019/121394) The present invention relates to solid forms of the insecticide of formula (I): compositions comprising the solid forms and methods of their use as insecticides.
机翻摘要
暂无翻译结果,您可以尝试点击头部的翻译按钮。
地址
代理人
(WO2019121394) SYNGENTA INTERNATIONAL AG ([CH])
代理机构
;
优先权号
2017GB-0021235
主权利要求
(WO2019/121394) Claims 1. A crystalline polymorph of the compound of formula IA  which has a powder X-ray diffraction pattern comprising at least three 2Q angle values selected from the group consisting of 6.0 ± 0.2, 8.8 ± 0.2, 9.4 ± 0.2, 10.1 ± 0.2, 11.9 ± 0.2, 14.5 ± 0.2, 15.9 ± 0.2, 20.2 ± 0.2, 20.7 ± 0.2, 21.2 ± 0.2, 21.7 ± 0.2, 22.1 ± 0.2 and 22.7 ± 0.2. 2. The crystalline polymorph of claim 1, which has the following lattice parameters: a=5.06 A ± 0.01 A, b=l8.92 A ± 0.01 A, c=24.l7 A ± 0.01 A, a = 90° ± 0.01 °, b = 90°  ± 0.01 °, g = 90° ± 0.010and volume = 2315A3± 1 A3 . 3. The crystalline polymorph of claim 1 or claim 2, which has a melting point of l4l°C ± 2°C. 4. A crystalline polymorph of the compound of formula IA, which is a hydrate and which has a powder X-ray diffraction pattern comprising at least three 20 angle values selected from the group consisting of 4.4 ± 0.2, 7.0 ± 0.2, 8.7 ± 0.2, 10.3 ± 0.2, 11.0 ± 0.2, 12.4 ± 0.2, 12.7 ± 0.2, 13.3 ± 0.2, 14.1 ± 0.2, 15.9 ± 0.2, 17.1 ± 0.2, 18.6 ± 0.2, 19.0 ± 0.2 and 19.6 ± 0.2. 5. The crystalline polymorph of claim 4, which has the following lattice parameters: a=8.03 A ± 0.01 A, b=l6.10 A ± 0.01 A, c=20.37 A ± 0.01 A, a = 90° ± 0.01 °, b =  97.02° ± 0.01 °, g = 90° ± 0.010and volume = 2615A3± 1 A3 . 6. A crystalline polymorph of the compound of formula IB or IC  which has a powder X-ray diffraction pattern comprising at least three 2Q angle values selected from the group consisting of 4.1 ± 0.2, 8.3 ± 0.2, 10.2 ± 0.2, 12.4 ± 0.2, 15.5 ± 0.2, 16.5 ± 0.2, 18.2 ± 0.2, 18.4 ± 0.2, 18.7 ± 0.2, 19.0 ± 0.2, 20.5 ± 0.2, 21.0 ± 0.2 and 21.4 ± 0.2. 7. The crystalline polymorph of claim 6, which has a melting point of 206°C ± 2°C. 8. A crystalline polymorph of the racemate of the compounds of formula IA and ID  which has a powder X-ray diffraction pattern comprising at least three 20 angle values selected from the group consisting of 4.0 ± 0.2, 8.1 ± 0.2, 9.7 ± 0.2, 11.1 ± 0.2, 12.7 ± 0.2, 15.3 ± 0.2, 15.9 ± 0.2, 16.2 ± 0.2, 16.7 ± 0.2, 18.4 ± 0.2, 19.5 ± 0.2, 19.8 ± 0.2, 20.3 ± 0.2, 21.8 ± 0.2 and 23.9 ± 0.2. 9. The crystalline polymorph of claim 8, which has a melting point of l73°C ± 2°C. 10. An agricultural composition comprising a polymorph as claimed in any one of claims 1 to 9 and at least one agriculturally acceptable carrier or diluent. 11. The composition of claim 10, which comprises more than one polymorph of the   polymorphs defined in any one of claims 1 to 9. 12. The composition of claim 10, which is enriched for a polymorph of the compound of formula IA. 13. The composition of claim 12, which is enriched for the polymorph as defined in claims 1 to 3. 14. The composition of any one of claims 10 to 13, which comprises at least one further insecticide or nematicide. 15. A method of preventing or controlling insect infection on plants or plant propagation material comprising treating the plant or plant propagation material with an   insecticidally effective amount of an agricultural composition as claimed in any one of claims 10 to 14.
法律状态
PENDING
专利类型码
A1
国别省市代码
若您需要申请原文,请登录。

最新评论

暂无评论。

登录后可以发表评论

意见反馈
返回顶部